Steklo i Keramika (Glass and Ceramics). Monthly scientific, technical and industrial journal

 

ISSN 0131-9582 (Online)

  • Continuous numbering: 1109
  • Pages: 3-13
  • Share:

Heading: Not-set

Ceramics in the Ca 2 P 2 O 7 -Ca (PO 3 ) 2 was obtained by firing a cement stone made from a powder mixture containing ?-tricalcium phosphate ?-Ca 3 (PO 4 ) 2 and monocalcium phosphate monohydrate Ca (H 2 PO 4 ) 2 & middot; Н 2 O. The Ca / P molar ratio of the starting powder mixtures was set to Ca / P & lt; 1. According to XRD data, all ceramic samples after firing at 1000 ° C included ?-calcium pyrophosphate ?-Ca 2 P 2 O 7 , and a ceramic sample from a powder mixture with a maximum content of monocalcium phosphate monohydrate Ca (H 2 PO 4 ) 2 & middot; H 2 O contained also ?-calcium polyphosphate ?-Ca (PO 3 ) 2 . The resulting calcium phosphate ceramics with a low firing temperature can be used to create a resorbable base for tissue engineering structures.
Cand. tech. Sciences T. V. SAFRONOVA 1 ( e-mail: This email address is being protected from spambots. You need JavaScript enabled to view it. ), Cand. physical-mat. Sci. S. A. KORNEYCHUK 1 , Cand. chem. Sciences T. B. Shatalova 1 , Cand. tech. Sci. Yu. S. LUKINA 2 , Cand. tech. Sci. S. P. SIVKOV 2 , Cand. chem. Sci. Y. YU. FILIPPOV 1 , Cand. chem. Sci. V. K. KRUTKO 3 , Cand. chem. sciences ON MUSSKAYA 3 ;
1 Moscow State University named after MV Lomonosov (Russia, Moscow)
2 Russian University of Chemical Technology. D. I. Mendeleeva (Russia, Moscow)
3 Institute of General and Inorganic Chemistry of the National Academy of Sciences of Belarus (Belarus, Minsk)
Winkler T., Sass FA, Duda GN, Schmidt-Bleek K. A review of biomaterials in bone defect healing, remaining shortcomings and future opportunities for bone engineering tissue : The unsolved challenge // Bone & Joint Research. 2018. V. 7. No. 3.P. 232? 243. URL: https://doi.org/10.1302/2046-3758.73.BJR2017-0270.R1 Li JJ, Ebied M., Xu J., Zreiqat H. Current Approaches to Bone Tissue Engineering: The Interface between Biology and Engineering // Advanced healthcare materials. 2018. V. 7. No. 6. P. 1701061. URL: https: // doi.org/10.1002/adhm.201701061 Lee JH, Chang BS, Jeung UO et al. The first clinical trial of beta-calcium pyrophosphate as a novel bone graft extender in instrumented posterolateral lumbar fusion // Clinics in orthopedic surgery, 2011. V. 3. No. 3.P. 238? 244. URL: https://doi.org/10.4055/cios. 2011.3.3.238 Toshima T., Hamai R., Tafu M. et al. Morphology control of brushite prepared by aqueous solution synthesis // Journal of Asian Ceramic Societies. 2014. V. 2. No. 1. of P. 52? 56. URL: https://doi.org/10.1016/j.jascer. 2014.01.004 Arifuzzaman SM, Rohani S. Experimental study of brushite precipitation // Journal of Crystal Growth. 2004. V. 267. No. 3? 4.P. 624? 634. URL: https://doi.org/ 10.1016 / j.jcrysgro.2004.04.024 Tas AC Monetite (CaHPO4) synthesis in ethanol at room temperature // Journal of the American Ceramic Society. 2009. V. 92. No. 12.P. 2907? 2912. URL: https://doi.org/10.1111/j.1551-2916.2009.03351.x Thomas G., Dehbi H. Effect of water on monetite synthesis in the solid state // Materials chemistry and physics. 1986. V. 15. No. 1.P. 1? 13. URL: https: // doi.org/10.1016/0254-0584(86)90084-2 Safronova T.V., Putlyaev V.I., Kurbatova S.A. et al. Properties of amorphous calcium pyrophosphate powder synthesized using ion exchange to obtain bioceramics // Inorganic materials. 2015.Vol. 51.? 11, p. 1269? 1276. URL: https://doi.org/10.7868/S0002337X15110093 Safronova T.V., Kurbatova S.A., Shatalova T.B. et al. Calcium pyrophosphate powder synthesized from pyrophosphoric acid and calcium acetate for the production of bioceramics // Materials Science. 2016.? 7, p. 41? 48. Kukueva EV, Putlyaev VI, Safronova TV, Tikhonov AA Composite bioceramics based on decomposition products of octacalcium phosphate // Glass and Ceramics. 2017.? 2.S. 37? 42. [Kukueva EV, Putlyaev VI, Safronova TV, Tikhonov AA Composite Bioceramic Based on Octacalcium Phosphate Decomposition Products // Glass Ceram. 2017. V. 74. No. 1 ? 2. P. 67? 72. URL: http://dx.doi.org/ 10.1007 / s10717-017-9931-2] Safronova T. V., Putlyaev V. I., Ivanov V. K. et al. Powder mixtures based on ammonium hydrogen phosphate and calcium carbonate for the production of biocompatible porous ceramics in the CaO? P2O5 system // New refractories. 2015.? 9, p. 45? 53. Safronova TV, Shatalova TB, Filippov Ya. Yu. Et al. Ceramics in the Ca2P2O7? Ca (PO3) 2 system obtained by firing samples from hardening mixtures based on calcium citrate and monocalcium phosphate monohydrate // Materials Science. 2019.? 9.C. 31? 40. URL: http://dx.doi.org/10.31044/1684-579X-2019-0-9-31-40 Gbureck U., Hellzel T., Biermann I. et al. Preparation of tricalcium phosphate / calcium pyrophosphate structures via rapid prototyping // Journal of Materials Science: Materials in Medicine. 2008. V. 19. No. 4.P. 1559? 1563. URL: https://doi.org/10.1007/s10856-008-3373-x Bolarinwa A., Gbureck U., Purnell P. et al. Cement casting of calcium pyrophosphate based bioceramics // Advances in Applied Ceramics. 2010. V. 109. No. 5. of P. 291? 295. URL: https://doi.org/10.1179/ 174367609X459586 Safronova T.V., Lukina Yu.S., Sivkov S.P. et al. Ceramics based on calcium pyrophosphate obtained by firing cement stone // Technique and technology silicates. 2020.Vol. 27.? 1.S. 17? 20. Safina NM, Safronova TV, Lukin ES Ceramics based on calcium phosphates with low sintering temperature, containing a resorbable phase. Glass and Ceramics. 2007.? 7, p. 19? 24. [Safina MN, Safronova TV, Lukin ES Calcium phosphate based ceramic with a resorbable phase and low sintering temperature // Glass Ceram. 2007. V. 64. No. 7-8. P. 238? 243. URL: http://dx.doi.org/10.1007/ s10717-009-9086-x] Wang K., Chen F., Liu C., R? Ssel C. The effect of polymeric chain-like structure on the degradation and cellular biocompatibility of calcium polyphosphate // Materials Science and Engineering: C. 2008. V. 28. No. 8.P. 1572? 1578. URL: https://doi.org/10.1016/ j.msec. 2008.04.017 Jackson LE, Wright AJ A New Synthetic Route to Calcium Polyphosphates // Key Engineering Materials. 2005. V. 284. P. 71? 74. URL: https://doi.org/10.4028/ www.scientific.net/KEM.284-286.71 Trommer J., Schneider M., Worzala H., Fitch AN Structure determination of CaH2P2O7 from in situ powder diffraction data / / Materials Science Forum. 2000. V. 321. P. 374? 379. URL: https://doi.org/10.4028/www. scientific.net/MSF.321-324.374 Brown EH, Brown WE, Lehr JR et al. Calcium ammonium pyrophosphates // The Journal of Physical Chemistry. 1958. V. 62. No. 3.R. 366? 367. URL: https://doi.org/10.1021/j150561a036 Subbarao YV, Ellis R. Reaction products of polyphosphates and orthophosphates with soils and influence on uptake of phosphorus by plants // Soil Science Society of America Journal. 1975. V. 39. No. 6.R. 1085? 1088. URL: https://doi.org/10.2136/sssaj1975.03615995003900060022x Brown EH, Lehr JR, Smith JP, Frazier AW Fertilizer Materials, Preparation and Characterization of Some Calcium Pyrophosphates // Journal of Agricultural and Food Chemistry. 1963. V. 11. No. 3.P. 214? 222. URL: https://doi.org/10.1021/jf60127a020 Zobel D., Ba N. Untersuchungen zur Phosphitpyrolyse; Reaktionen beim Erhitzen von CaH2 (HPO3) 2 H2O in Abwesenheit von Sauerstoff // Z. Chem. 1969. V. 9. No. 11.P 433. URL: https://doi.org/10.1002/zfch. 19690091118 Safronova TV, Mukhin EA, Putlyaev VI et al. Amorphous calcium phosphate powder synthesized from calcium acetate and polyphosphoric acid for bioceramics application // Ceramics International. 2017. V. 43. P. 1310? 1317. URL: http://dx.doi.org/10.1016/ j.ceramint.2016.10.085 Safronova T.V., Kiselev A.S., Shatalova T.B. et al. Synthesis of calcium / ammonium double pyrophosphate monohydrate Ca (NH4) 2P2O7 • H2O? precursor of biocompatible phases of calcium phosphate ceramics // Izvestiya Akademii Nauk. Ser. chemical. 2020.? 1.P. 139? 147. MacLennan G., Beevers CA The crystal structure of monocalcium phosphate monohydrate, Ca (H2PO4) 2 • H2O // Acta Crystallographica. 1956. V. 9. No. 2.P. 187? 190. URL: https://doi.org/10.1107/S0365110X56000413 Boonchom B., Danvirutai C. The morphology and thermal behavior of Calcium dihydrogen phosphate monohydrate (Ca (H2PO4) 2 • H2O) obtained by a rapid precipitation route at ambient temperature in different media // J. Optoelectron. Biomed. Mater. 2009. V. 1. P. 115? 123. URL: http://chalcogen.ro/1Boonchom1.pdf Boonchom B. Parallelogram-like microparticles of calcium dihydrogen phosphate monohydrate (Ca (H2PO4) 2H2O) obtained by a rapid precipitation route in aqueous and acetone media // Journal of alloys and compounds. 2009. V. 482. No. 1 ? 2.P. 199? 202. URL: https: // doi.org/10.1016/j.jallcom.2009.03.157 Safronova T.V., Putlyaev V.I., Knot'ko A.V. et al. Calcium phosphate ceramics in the Ca (PO3) 2 system ? Ca2P2O7 based on a powder mixture containing calcium hydrogen phosphates // Glass and ceramics. 2018. ? 7.C. 37? 44. ? Safronova TV, Putlyaev VI, Knot? Ko AV et al. Calcium Phosphate Ceramic in the System Ca (PO3) 2? Ca2P2O7 Based on Powder Mixtures Containing Calcium Hydrophosphate // Glass Ceram. 2018. V. 75. No. 7-8. P. 279? 286. URL: http://dx.doi.org/10.1007/s10717-018-0072-z? Filippov YY, Orlov ED, Klimashina ES et al. Colloidal forming of macroporous calcium pyrophosphate bioceramics in 3D-printed molds // Bioactive Materials. 2020. V. 5. No. 2.P. 309? 317. Lode A., Meissner K., Luo Y. et al. Fabrication of porous scaffolds by three? Dimensional plotting of a pasty calcium phosphate bone cement under mild conditions // Journal of tissue engineering and regenerative medicine. 2014. V. 8. No. 9.P. 682? 693. URL: https://doi.org/ 10.1002 / term.1563 ICDD (2010). PDF-4 + 2010 (Database) / ed. by Dr. Soorya Kabekkodu; International Center for Diffraction Data. Newtown Square. PA. USA, 2010. URL: http: // www.icdd.com/products/pdf2.htm Hill WL, Faust GT, Reynolds DS System CaO? P2O5 // Am. J. Sci. 1944. V. 242. No. 9.P. 457? 477. url: http://dx.doi.org/10.2475/ajs.242.9.457

The article can be purchased
electronic!

PDF format

700 руб

UDK 666.3:546.41:661.635.41
Article type: Not-set
Make a request

Keywords

Use the reference below to cite the publication

Safronova T. V., Korneychuk S. A., Shatalova T. B., Lukina Yu. S., Sivkov S. P., Filippov Ya. Yu., Krutko V. K., Musskaya O. N. Ceramics in the Са2Р2О7-Са(РО3)2 System Obtained by Firing of Cement Stone Based on β-tricalcium Phosphate and Monocalcium Phosphate Monohydrate. Steklo i keramika. 2020:93(5):3-13. (in Russ). UDK 666.3:546.41:661.635.41