Steklo i Keramika (Glass and Ceramics). Monthly scientific, technical and industrial journal

 

ISSN 0131-9582 (Online)

  • Continuous numbering: 1117
  • Pages: 9-15
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A method for obtaining high-purity tungsten (VI) oxide based on two-stage sublimation purification has been developed. An impurity analysis of commercial preparations of tungsten (VI) oxide by inductively coupled plasma mass spectrometry was carried out. KGW crystals were obtained, grown using commercial reagents and tungsten (VI) oxide with a chemical purity of 99.999 & # 37; by mass. A comparative analysis of crystals grown from various initial tungsten oxides has been carried out. It is shown that the developed high-purity tungsten (VI) oxide does not reduce the chemical purity of the grown KGW crystals and is a promising raw material for the technology of glass-ceramic optical materials based on tungstates.
A. V. KHOMYAKOV 1 , Cand. chem. Sciences E. N. MOZHEVITINA 1 , Cand. chem. M. P. ZYKOVA 1 , Cand. tech. Sciences AM YURKIN 2 , Dr. Sciences I. Kh. AVETISOV 1 (This email address is being protected from spambots. You need JavaScript enabled to view it.); 1 Federal State Budgetary Educational Institution of Higher Education & # 171; Russian Chemical-Technological University named after V.I. D. I. Mendeleev & # 187; (RKhTU named after D. I. Mendeleev) (Russia, Moscow)
2 CJSC & # 171; Siberian single crystal & ndash; EKSMA & # 187; (Russia, Novosibirsk)
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KHOMYAKOV A. V., MOZHEVITINA E. N., ZYKOVA M. P., AVETISS-OV I. CH., YURKIN A. M. High Purity Tungsten (VI) Oxide for Producing Advanced Laser Materials. Steklo i keramika. 2021:94(1):9-15. (in Russ). UDK 666.3:661.692:661.657.1:54-482