Steklo i Keramika (Glass and Ceramics). Monthly scientific, technical and industrial journal

 

ISSN 0131-9582 (Online)

  • Continuous numbering: 1183
  • Pages: 10-17
  • Share:

Heading: Not-set

The effect of electron-beam sintering in the fore-vacuum pressure range (8…10 Pa) on the density, structure, and phase composition of the sintered Al2O3–Cu composite with a component mass ratio of 10:1 was investigated. It was established that the maximum density of the sintered composite (2.85 g/cm3) is achieved at a temperature of 1300 °C. It was also shown that upon heating above 1100 °C, copper migrates to the surface and evaporates, forming a depleted near-surface layer. The metallic Cu phase was detected only at 1100 °C (2 wt. %), whereas at higher temperatures only traces of CuO were present. The obtained results confirm the feasibility of producing gradient Al2O3–Cu structures using this method.
Aleksandr S. Klimov – Doctor of Technical Sciences, Professor, Department of Physics, Tomsk State University of Control Systems and Radioelectronics, Tomsk, Russia
Ilya Yu. Bakeev – Associate Professor, Department of Physics, Tomsk State University of Control Systems and Radioelectronics, Tomsk, Russia
Sergey A. Enduraev – student, Department of Physical Electronics, Tomsk State University of Control Systems and Radioelectronics, Tomsk, Russia
Aleksey A. Zenin – Associate Professor, Department of Physics, Tomsk State University of Control Systems and Radioelectronics, Tomsk, Russia
Oksana V. Fyodorova – Associate Professor, Department of Physics, Tomsk State University of Control Systems and Radioelectronics, Tomsk, Russia
1. Dash K., Ray B. C., Chaira D. Synthesis and characterization of copper–alumina metal matrix composite by conventional and spark plasma sintering // Journal of Alloys and Compounds. 2012. V. 516. P. 78 – 84.
2. Barakat W. S., Habba M. I., Ibrahim A., et al. The effect of Cu coated Al2O3 particle content and densification methods on the microstructure and mechanical properties of Al matrix composites // Journal of Materials Research and Technology. 2023. V. 24. P. 6908 – 6922.
3. Fathy A., Shehata F., Abdelhameed M., Elmahdy M. Compressive and wear resistance of nanometric alumina reinforced copper matrix composites // Materials & Design. 2012. V. 36. P. 100 – 107.
4. Koraс M., Anвiс Z., Tasiс M., Kamberoviс Z. Sintering of Cu–Al2O3 nano-composite powders produced by a thermochemical route // Journal of the Serbian Chemical Society. 2007. V. 72, No. 11. P. 1115 – 1125.
5. Yan Z. Q., Chen F., Ye F. X., et al. Microstructures and properties of Al2O3 dispersion-strengthened copper alloys prepared through different methods // International Journal of Minerals, Metallurgy and Materials. 2016. V. 23, No. 12. P. 1437 – 1443.
6. Chen Y., Ud-Din R., Yang T., et al. Preparing and wear-resisting property of Al2O3/Cu composite material enhanced using novel in situ generated Al2O3 nanoparticles // Materials. 2023. V. 16, No. 13. P. 4819.
7. Need R. F., Alexander D. J., Field R. D., et al. The effects of equal channel angular extrusion on the mechanical and electrical properties of alumina dispersion-strengthened copper alloys // Materials Science and Engineering A. 2013. V. 565. P. 450.
8. Rajkovic V., Bozic D., Devecerski A., Jovanovic M. T. Characteristic of copper matrix simultaneously reinforced with nano- and micro-sized Al2O3 particles // Materials Characterization. 2012. V. 67. P. 129.
9. Strojny-Nedza A., Pietrzak K., Weglewski W. The influence of Al2O3 powder morphology on the properties of Cu-Al2O3 composites designed for functionally graded materials (FGM) // Journal of Materials Engineering and Performance. 2016. V. 25, No. 8. P. 3173 – 3184.
10. Gupta M., Lai M. O., Srivatsan T. S. Synthesis and characterization of a free-standing, one-dimensional, Al–Cu/SiC-based functionally graded material // Journal of Materials Synthesis and Processing. 2002. V. 10, No. 2. P. 75 – 81.
11. Hwang S. J., Lee J. Mechanochemical synthesis of Cu–Al2O3 nanocomposites // Materials Science and Engineering A. 2005. V. 405, No. 1–2. P. 140.
12. Lee J., Kim Y. C., Lee S., et al Correlation of the microstructure and mechanical properties of oxide-dispersion-strengthened copper fabricated by internal oxidation // Metallurgical and Materials Transactions A. 2004. V. 35, No. 2. P. 493.
13. Feng T., Zheng W., Chen W., et al Enhanced interfacial wettability and mechanical properties of Ni@Al2O3/Cu ceramic matrix composites using spark plasma sintering of Ni coated Al2O3 powders // Vacuum. 2021. V. 184. P. 109938.
14. Liang S., Fan Z., Xu L., Fang L. Kinetic analysis on Al2O3/Cu composite prepared by mechanical activation and internal oxidation // Composites Part A: Applied Science and Manufacturing. 2004. V. 35, No. 12. P. 1441 – 1446.
15. Zygmuntowicz J., Los J., Kurowski B., et al. Investigation of microstructure and selected properties of Al2O3–Cu and Al2O3–Cu–Mo composites // Advanced Composites and Hybrid Materials. 2021. V. 4, No. 1. P. 212 – 222.
16. Shi Y., Chen W., Dong L., et al. Enhancing copper infiltration into alumina using spark plasma sintering to achieve high performance Al2O3/Cu composites // Ceramics International. 2018. V. 44, No. 1. P. 57 – 64.
17. Klimov A., Bakeev I., Oks E., Zenin A. Electron beam sintering of composite Al2O3–ZrO2 ceramics in the forevacuum pressure range // Coatings. 2022. V. 12, No. 2. P. 278.
18. Klimov A., Bakeev I., Dolgova A., et al. Electron-beam sintering of Al2O3–Cr-based composites using a forevacuum electron source // Ceramics. 2022. V. 5, No. 4. P. 748 – 760.
19. Surzhikov A. P., Frangulyan T. S., Ghyngazov S. A., et al. Sintering of zirconia ceramics by intense high-energy electron beam // Ceramics International. 2016. V. 42, No. 12. P. 13888 – 13892.
20. Zenin A. A., Bakeev I. Y., Klimov A. S., Oks E. M. Powerful electron beam transport from a plasma–cathode electron source at forevacuum pressure // Plasma Sources Science and Technology. 2021. V. 30, No. 3. P. 035007.
21. Tyunkov A. V., Klimov A. S., Savkin K. P., et al. Electron-beam deposition of metal and ceramic-based composite coatings in the fore-vacuum pressure range // Ceramics. 2022. V. 5, No. 4. P. 789 – 797.

The article can be purchased
electronic!

PDF format

700 руб.

DOI: 10.14489/glc.2026.07.pp.010-017
Article type: Research Article
Make a request

Keywords

Use the reference below to cite the publication

Klimov A. S., Bakeev I. Yu., Enduraev S. A., Zenin A. A., Fedorova O. V. Electron beam sintering of alumina-based composite ceramics with copper addition in the fore-vacuum pressure range. Steklo i keramika. 2026:99(7):10-17. (in Russ). DOI: 10.14489/glc.2026.07.pp.010-017