One of the main disadvantages of sulfur concrete is the formation of a crack defect when cooled in metal molds. The proposed way of using sequential addition of components, temperature control at the entire mixing stage of the mixture is based on previous studies, which showed that the main factors determining the compressive strength of samples are both sulfur itself and its interaction with fine filler, as well as its strength properties. The work is devoted to determining the influence of technological factors and methods of preparing mineral components on the strength of sulfur-concrete samples. To prepare sulfur-concrete samples, ground industrial sulfur produced by Kaspiigaz LLC, natural zeolite of the Kempendyaysky field, and crushing waste from carbonate rocks of the Sasaabytsky field were used. For experimental studies, compositions were prepared with the following content: ground sulphur 30 wt. %, filled with fine zeolite powder in amount of 5 wt. % and limestone crushed stone screening – 65 wt. %, using three methods of preparing mineral components. For mixing, a developed forced mixer was used, which provided an upper load of raw materials and unloading of the finished sulfur-concrete mixture. The determination of the compressive strength of sulfur-concrete samples was carried out on an IP-1A-1000 test machine, structural studies of samples were carried out on a JEOL JSM-6480LV high-resolution scanning electron microscope. A scheme of a mixing installation is proposed, which made it possible to optimize the multivariable stages of preparing a mixture for making sulfur-concrete samples due to the special shape of the blades and their location on the rotating shaft, as well as uniform heating of the mixture, high-quality mixing of ingredients is ensured to obtain a homogeneous technological mixture, the properties of which are the same in any individual volume. A method has been selected that makes it possible to produce sulfur-concrete samples without defects and increase the compressive strength by 17 %.
Lira A. Nikolaeva – Candidate of Technical Sciences, senior researcher, Laboratory of Composite Building Materials, Federal Research Center "Yakut Scientific Center of Siberian Branch of the Russian Academy of Sciences", a Separate Division Institute of Oil and Gas Problems SB RAS, Yakutsk, Russia
Maria E. Savvinova – Candidate of Technical Sciences, senior researcher, Laboratory of Composite Building Materials, Federal Research Center "Yakut Scientific Center of Siberian Branch of the Russian Academy of Sciences", a Separate Division Institute of Oil and Gas Problems SB RAS, Yakutsk, Russia
Aitalina A. Andreeva – junior researcher, Laboratory of Composite Building Materials, Federal Research Center "Yakut Scientific Center of Siberian Branch of the Russian Academy of Sciences", a Separate Division Institute of Oil and Gas Problems SB RAS, Yakutsk, Russia
1. Khan S. H., Amani S., Amani M. Alternative and potential uses for the sulfur byproducts produced from oil and gas fields // International Journal of Organic Chemistry. 2021. V. 11, Nо. 1. Р. 14 – 23. DOI: 10.4236/ijoc.2021.111002
2. Wagenfeld J.-G., Al-Ali K., Almheiri S., et al. Sustainable applications utilizing sulfur, a by-product from oil and gas industry: a state-of-the-art review // Waste Management. 2019. V. 95. Р. 78 – 89. DOI: 10.1016/j.wasman.2019.06.002
3. Yakovlev G. I., Polyanskih I. S., Gordina A. F., et al. Using technical sulfur as a structuring additive for mineral binders based on calcium sulfate // Engineering Structures and Technologies. 2020. V. 11. Р. 95 – 100. DOI: 10.3846/est.2019.11948
4. Фомин А. Ю., Аскарова Р. Н., Хозин В. Г. Высокопрочный серощебень из карбонатных пород для устройства оснований в конструкциях дорожных одежд // Известия Казанского государственного архитектурно-строительного университета. 2022. № 1(59). С. 54 – 63. DOI: 10.52409/20731523_2022_1_54
5. Leskin A. I., Aleksikov S. V., Gofman D. I. Organic composite binder improving the physical and mechanical properties of low-strength stone materials // IOP Conference Series: Materials Science and Engineering. 2021. V. 965. Р. 2 – 22. DOI: 10.1088/1757-899X/962/2/022002
6. Le H. T., Korolev E. V., Grishina A. N., Gladkikh V. A. Reasons for reduced moisture resistance of sulfur-extended asphalt concrete // Materials. 2021. V. 14, Nо. 23. Р. 45 – 53. DOI: 10.31659/0585-430X-2021-789-3-39-44
7. Миронов Н. С., Васильев А. Ю. Серобетон – перспективный материал для транспортного строительства // Транспортное строительство. 2023. № 3. С. 14–15.
8. Ziyamukhamedova U., Bakirov L., Donaev S., et al. Study of structure formation processes in matrices of mixed components with reinforcing natural fillers // E3S Web of Conferences. 2023. V. 401. Р. 05074. DOI: 10.1051/e3sconf/202340105074
9. Миронов Н. С., Васильев А. Ю. Особенности применения композитных материалов на основе модифицированной серы в Арктике // Фундаменты. 2023. № 3. С. 61 – 63.
10. Сагадеев Е. В., Сулейманова Л. А., Ибрагимов Р. А., Сагадеев В. В. Получение и исследование физико-механических свойств композиций серных бетонов // Вестник Белгородского государственного технологического университета им. В. Г. Шухова. 2025. № 7. С. 8 – 19. DOI: 10.34031/2071-7318-2025-10-7
11. Fediuk R., Amran Y. H. M., Mosaberpanah M. A., et al. Critical review on the properties and applications of sulfur-based concrete // Materials. 2020. V. 13. Р. 1 – 23 DOI: 10.3390/ma13214712
12. Фомин А. Ю., Гафиятуллин Г. Р., Низамутдинов Р. И. Модифицированный серный бетон на основе карбонатных заполнителей для производства изделий // Автомобильные дороги и транспортная инфраструктура. 2024. № 4(8). С. 18 – 25.
13. Личман Н. В. К вопросу о терминах «серное связующее» и «серное вяжущее» в серосодержащих композиционных материалах // Строительные материалы. 2018. № 12. С. 76 – 80. DOI: 10.31659/0585-430X-2018-766-12-76-80
14. Ашимова С., Елшибаев А. Технология получения высокопрочного серощебня для дорожного строительства в Республике Казахстан // Вестник КазАТК. 2022. № 122(3). С. 26 – 32. DOI: 10.52167/1609-1817-2022-122-3-26-32
15. Урханова Л. А., Мослемани И. Ж. Улучшение физико-механических свойств цементного камня с использованием высокодисперсной серы // Цемент и его применение. 2025. № 2. С. 67 – 69.
16. Иванов А. А., Урханова Л. А., Лхасаранов С. А., Хардаев П. К. Исследование влияния тонкодисперсных добавок на свойства композиционных вяжущих для гидротехнического бетона // Вестник ВСГУТУ. 2023. № 2(89). С. 80 – 88. DOI: 10.53980/24131997_2023_2_80
17. Аманова Н. Д., Тураев Х. Х., Бекназаров Х. С. Синтез и исследование свойства модифицированной серы и серобетона // Технические науки. 2021. № 11-3(80). С. 15 – 21.
18. Mozgawa W. The influence of some heavy metals cations on the FTIR spectra of zeolites // Journal of Molecular Structure. 2000. V. 555. P. 299 – 304.
19. Yan P., Zhao W., Tonkin S. J., Chalker J. M., et al. Stretchable and durable inverse vulcanized polymers with chemical and thermal recycling // Chemistry of Materials. 2022. V. 34. Р. 1167 – 1178. DOI: 10.1021/acs.chemmater.1c03662
20. Mozgawa W. The relation between structure and vibrational spectra of natural zeolites // Journal of Molecular Structure. 2001. V. 596. P. 129 – 137.
21. Tulaev Sh., Amanova N., Beknazarov Kh. Study of sulfur modification with unsaturated compounds // ISJ Theoretical & Applied Science. 2022. V. 109. Р. 283 – 286. DOI: 10.15863/TAS.2022.05.109.26
The article can be purchased
electronic!
PDF format
700 руб
DOI: 10.14489/glc.2026.09.pp.055-062
Article type:
Research Article
Make a request